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Procedures for Testing and |
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Provision, Source
Category, or Test Method |
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| Cover Page |  |
| Table of Contents | |
| Introduction | |
Test Report Transmission Summary |
 |
| PART I: GENERAL PROVISIONS | |
| Section 1.1 - Applicability | |
| Section 1.2 - Performance and Compliance Testing | |
| Section 1.3 - Compliance with Standards and Maintenance Requirements | |
| Section 1.4 - Monitoring Requirements | |
| Section 1.5 - Notification and Record Keeping | |
| Section 1.6 - Incorporations by Reference | |
| Section 1.7 - General Control Device Requirements | |
| Section 1.8 - Required Overall Emissions Reduction Efficiency | |
| Section 1.9 - General Notification and Reporting Requirements | |
| PART II: SOURCE CATEGORIES | |
| Section 2.1 - Fuel Burning Equipment | |
| Section 2.1b - Industrial-Commercial-Institutional Steam Generating (Constructed after June 19, 1984) | |
| Section 2.1c - Small Industrial-Commercial-Institutional Steam Generating Units (NSPS) | |
| Section 2.2 - Incinerators | |
| Section 2.2a - Municipal Waste Combustors | |
| Section 2.2b - Municipal Waste Combustors | |
| Section 2.3 - Portland Cement Plants | |
| Section 2.4 - Nitric Acid Plants | |
| Section 2.5 - Sulfuric Acid Plants | |
| Section 2.6 - Asphalt Concrete Plants | |
| Section 2.7 - Petroleum Refineries | |
| Section 2.8 - Storage Vessels for Petroleum Liquids and External Floating Roof Tanks | |
| Section 2.8a - Storage Vessels for Petroleum Liquids (Constructed after May 18, 1978) | |
| Section 2.8b - Volatile Organic Liquid Storage Vessels (Including Petroleum Liquid Storage Vessels - after July 23, 1984) | |
| Section 2.9 - Secondary Lead Smelters | |
| Section 2.10 - Secondary Brass and Bronze Ingot Production Plants | |
| Section 2.11 - Iron and Steel Plants | |
| Section 2.11a - Iron and Steel Plants (Secondary Emissions) | |
| Section 2.12 - Sewage Treatment Plants | |
| Section 2.13 - Primary Copper Smelters | |
| Section 2.14 - Primary Zinc Smelters | |
| Section 2.15 - Primary Lead Smelters | |
| Section 2.16 - New Primary Aluminum Reduction Plants | |
| Section 2.22 - Coal Preparation Plants | |
| Section 2.23 - Ferroalloy Production Facilities | |
| Section 2.24 - Steel Plants: Electric Arc Furnaces | |
| Section 2.24a - Steel Plants: Electric Arc Furnaces and Argon-Oxygen Decarburization Vessels (Constructed after August 7, 1983) | |
| Section 2.25 - Metallurgical Melting - Cupola Furnaces | |
| Section 2.28 - Existing Kraft Pulp Mills | |
| Section 2.29 - New Kraft Pulp Mills | |
| Section 2.30 - Glass Manufacturing Plants | |
| Section 2.31 - Grain Elevators | |
| Section 2.33 - Surface Coating of Metal Furniture | |
| Section 2.34 - Stationary Gas Turbines | |
| Section 2.35 - Lime Manufacturing Plants | |
| Section 2.39 - Lead-Acid Battery Manufacturing Plants | |
| Section 2.40 - New Automobile and Light-Duty Truck Surface Coating Operations | |
| Section 2.42 - New Bulk Gasoline Terminals | |
| Section 2.43 - Paper Coating (All Sources) | |
| Section 2.44 - Graphic Arts Industry: Publication Rotogravure Printing (NSPS Sources) | |
| Section 2.45 - Graphic Arts Industry: All Sources | |
| Section 2.46 - Pressure Sensitive Tape and Label Surface Coating Operations (NSPS Sources) | |
| Section 2.47 - Metal Coil Coating | |
| Section 2.48 - Asphalt Processing and Asphalt Roofing Plants | |
| Section 2.49 - Equipment Leaks of VOC in the Synthetic Organic Chemicals Manufacturing Industry | |
| Section 2.50 - Industrial Surface Coating of Large Appliances | |
| Section 2.51 - Beverage Can Coating | |
| Section 2.52 - Surface Coating of Miscellaneous Metal Parts | |
| Section 2.53 - Wire Coating | |
| Section 2.54 - Rubber Tire Manufacturing Industry (NSPS Sources) | |
| Section 2.55 - Paper Coating Operations | |
| Section 2.59 - Flexible Vinyl and Urethane Coating and Printing | |
| Section 2.60 - Equipment Leaks of VOC in Petroleum Refineries | |
| Section 2.62 - Synthetic Organic Chemical Manufacturing Industry (SOCMI) - Air Oxidation Unit Processes | |
| Section 2.67 - Synthetic Organic Chemical Manufacturing Industry (SOCMI) - Distillation Operations | |
| Section 2.68 - Non-Metallic Mineral Processing Plants | |
| Section 2.69 - Wool Fiberglass Insulation Manufacturing Plants | |
| Section 2.73 - Surface Coating of Plastic Parts for Business Machines | |
| Section 2.74 - Calciners and Dryers in Mineral Industries | |
| Section 2.99 - Visible Emissions | |
| Section 2.100 - Granular and Mixed Fertilizer Manufacturing Plants | |
| Section 2.101 - Normal Superphosphate Facilities | |
| Section 2.102 - Kaolin and Fuller's Earth Manufacturing Processes | |
| Section 2.103 - Cotton Gins | |
| Section 2.104 - General Manufacturing Processes | |
| Section 2.105 - Ammonium Nitrate Fertilizer Processes | |
| Section 2.106 - Ammonium Sulfate Processes | |
| Section 2.107 - Metallic Mineral Processing Plants | |
| Section 2.108 - Synthetic Fiber Production Facilities | |
| Section 2.109 - Fabric and Vinyl Coating (All Sources) | |
| Section 2.110 - Gasoline Transport Vehicles | |
| Section 2.111 - Major Sources of VOC | |
| Section 2.112 - Automobile and Light-Duty Truck Surface Coating Operations (All Sources) | |
| Section 2.113 - Flat Wood Paneling | |
| Section 2.114 - Municipal Solid Waste Landfills | |
| Section 2.115 - Gasoline Dispensing Facility - Stage I and Stage II | |
| Section 2.116 - Electric Utility Steam Generation Units | |
| Section 2.117 - Hospital/Medical/Infectious Waste Incinerators (Constructed Before June 20, 1996) | |
| Section 2.118 - Aerospace Manufacturing and Rework Facilities | |
| Section 2.119 - Fuel Burning Equipment | |
| Section 2.120 - Stationary Gas Turbines and Stationary Engines used to Generate Electricity | |
| Section 2.121 - Large Stationary Gas Turbines | |
| Section 2.122 - Commercial & Industrial Solid Waste Incineration (Constructed before November 30, 1999) | |
| Section 2.123 - VOC Emissions from Extruded Polystyrene Products Manufacturing Utilizing an Injected Blowing Agent | |
| Section 2.124 - Multipollutant Control for Electric Utility Steam Generating Units | |
| Section 2.125 - Sulfur Dioxide Emissions from Electric Utility Steam Generating Plants | |
| Section 2.126 - Surface Coating of Miscellaneous Plastic Parts And Products | |
| Section 2.127 - Surface Coating of Miscellaneous Industrial Adhesives | |
| Section 2.128 - Surface Coating of Pleasure Craft | |
| Section 2.129 - VOC Emissions from Fiberglass Boat Manufacturing | |
| PART III: HAZARDOUS AIR POLLUTANTS | |
| Section 3.0 - General Provisions | |
| Section 3.1 - Asbestos | |
| Section 3.2 - Beryllium | |
| Section 3.4 - Mercury | |
| Section 3.5 - Ethylene Dichloride, Vinyl Chloride, and Polyvinyl Chloride Plants | |
| Section 3.21 - Equipment Leaks (Fugitive Emissions Sources) | |
| Section 3.27 - Benzene Transfer Operations | |
| PART IV: APPENDICES | |
| Appendix A - Part I - Test Methods: | |
| Method 1 - Sample and Velocity Traverses for Stationary Sources | |
| Method 1A - Sample and Velocity Traverses for Stationary Sources with Small Stacks or Ducts | |
| Method 2 - Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S Pitot Tube) | |
| Method 2A - Direct Measurement of Gas Volume through Pipes and Small ducts | |
| Method 2B - Determination of Exhaust Gas Volume Flow Rate from Gasoline Vapor Incinerators | |
| Method 2C - Determination of Stack Gas Velocity and Volumetric Flow Rate in Small Stacks or Ducts (Standard Pitot Tube) | |
| Method 2D - Measurement of Gas Volumetric Flow Rates in Small Pipes or Ducts | |
| Method 2E - Determination of Landfill Gas Production Flow Rate | |
| Method 2F - Determination of Stack Gas Velocity and Volumetric Flow Rate with Three-Dimensional Probes | |
| Method 2G - Determination of Stack Gas Velocity and Volumetric Flow Rate with Two-Dimensional Probes | |
| Method 2H - Determination of Stack Gas Velocity Taking into Account Velocity Decay Near the Stack Wall | |
| Method 3 - Gas Analysis for the Determination of Dry Molecular Weight | |
| Method 3A - Determination of Oxygen and Carbon Dioxide Concentrations in Emissions from Stationary Sources (Instrument Analyzer Procedure) | |
| Method 3B - Gas analysis for the Determination of Emission Rate correction Factor or Excess Air | |
| Method 3C - Determination of Carbon Dioxide, Methane, Nitrogen, and Oxygen from Stationary Sources | |
| Method 4 - Determination of Moisture Content in Stack Gases | |
| Method 5 - Determination of Particulate Emissions from Stationary Sources | |
| Method 5A - Determination of Particulate Emissions from the Asphalt Processing and Asphalt Roofing Industry | |
| Method 5D - Determination of Particulate Matter Emissions from Positive Pressure Fabric Filters | |
| Method 5E - Determination of Particulate Emissions from the Wool Fiberglass Insulation Manufacturing Industry | |
| Method 5F - Determination of Nonsulfate Particulate Matter from Stationary Sources | |
| Method 5T - Determination of Particulate Emissions from Stationary Sources - Total Dry and Wet Catch Method | |
| Method 6 - Determination of Sulfur Dioxide Emissions from Stationary Sources | |
| Method 6A - Determination of Sulfur Dioxide, Moisture, and Carbon Dioxide Emissions from Fossil Fuel Combustion Sources | |
| Method 6B - Determination of Sulfur Dioxide and Carbon Dioxide Daily Average Emissions from Fossil Fuel Combustion Sources | |
| Method 6C - Determination of Sulfur Dioxide Emissions from Stationary Sources (Instrumental Analyzer Procedure) | |
| Method 7 - Determination of Nitrogen Oxide Emissions from Stationary Sources | |
| Method 7A - Determination of Nitrogen Oxide Emissions from Stationary Sources (Ion Chromatography) | |
| Method 7B - Determination of Nitrogen Oxide Emissions from Stationary Sources (Ultraviolet Spectrophotometry) | |
| Method 7C - Determination of Nitrogen Oxide Emissions from Stationary Sources (Alkaline-Permanganate/Ion Colorimetric Method) | |
| Method 7D - Determination of Nitrogen Oxide Emissions from Stationary Sources (Alkaline-Permanganate/Ion Chromatographic Method) | |
| Method 7E - Determination of Nitrogen Oxide Emissions from Stationary Sources (Instrumental Analyzer Procedure) | |
| Method 8 - Determination of Sulfuric Acid Mist and Sulfur Dioxide Emissions from Stationary Sources | |
| Method 9 - Visual Determination of the Opacity of Emissions from Stationary Sources | |
| Method 10 - Determination of Carbon Monoxide Emissions from Stationary Sources | |
| Method 10A - Determination of Carbon Monoxide Emissions in Certifying Continuous Emission Monitoring Systems at Petroleum Refineries | |
| Method 10B - Determination of Carbon Monoxide Emissions from Stationary Sources | |
| Method 11 - Determination of Hydrogen Sulfide Content of Fuel Gas Streams in Petroleum Refineries | |
| Method 12 - Determination of Inorganic Lead Emissions from Stationary Sources | |
| Method 13A - Determination of Total Fluoride Emissions from Stationary Sources - SPANS Zirconium Lake Method | |
| Method 13B - Determination of Total Fluoride Emissions from Stationary Sources - Specific Ion Electrode Method | |
| Method 14 - Determination of Fluoride Emissions from Potroom Roof Monitors for Primary Aluminum Plants | |
| Method 15 - Determination of Hydrogen Sulfide, Carbonyl Sulfide, and Carbon Disulfide Emissions from Stationary Sources | |
| Method 15A - Determination of Total Reduced Sulfur Emissions from Sulfur Recovery Plants in Petroleum Refineries | |
| Method 16 - Semicontinuous Determination of Sulfur Emissions from Stationary sources | |
| Method 16A - Determination of Total Reduced Sulfur Emissions from Stationary Sources (Impinger Technique) | |
| Method 16B - Determination of Total Reduced Sulfur Emissions from Stationary Sources | |
| Method 17 - Determination of Particulate Emissions from Stationary Sources (In-Stack Filtration Method) | |
| Method 18 - Measurement of Gaseous Organic Compound Emissions by Gas Chromatography | |
| Method 19 - Determination of Sulfur Dioxide Removal Efficiency and Particulate Matter, Sulfur Dioxide, and Nitrogen Oxides Emission Rates | |
| Method 20 - Determination of Nitrogen Oxides, Sulfur Dioxide, and Oxygen Emissions from Stationary Gas Turbines | |
| Method 21 - Determination of Volatile Organic Compounds Leaks | |
| Method 22 - Visual Determination of Fugitive Emissions from Material Sources and Smoke Emissions from Flares | |
| Method 23 - Determination of Polychlorinated Dibenzo-p-Dioxins and Polychlorinated Dibenzofurans from stationary Sources | |
| Method 24 - Determination of Volatile Matter Content, Water content, Density, Volume Solids, and Weight Solids of Surface Coatings | |
| Method 24A - Determination of Volatile Matter Content and Density of Printing Inks and Related Coatings | |
| Method 25 - Determination of Total Gaseous Nonmethane Organic Emissions as Carbon | |
| Method 25A - Determination of Total Gaseous Organic Concentration Using a Flame Ionization Analyzer | |
| Method 25B - Determination of Total Gaseous Organic Concentration Using Nondispersive Infrared Analyzer | |
| Method 25C - Determination of Nonmethane Organic Compounds (NMOC) in MSW Landfill Gases | |
| Method 25D - Determination of the Volatile Organic Concentration of Waste Samples | |
| Method 25E - Determination of Vapor phase Organic Concentration in Waste Samples | |
| Method 26 - Determination of Hydrogen Chloride Emissions from Stationary Sources | |
| Method 26A - Determination of Hydrogen Halide and Halogen Emissions from Stationary Sources - Isokinetic Method | |
| Method 27 - Determination of Vapor Tightness of Gasoline Delivery Tank Using Pressure-Vacuum Test | |
| Method 29 - Determination of Metals Emissions from Stationary Sources | |
| Method 30A - Determination of Total Vapor Phase Mercury Emissions from Stationary Sources (Instrumental Analyzer Procedure) | |
| Method 30B - Determination of Total Vapor Phase Mercury Emissions from Coal-Fired Combustion Sources Using Carbon Sorbent Traps | |
| Method 101 - Determination of Particulate and Gaseous Mercury Emissions from Chlor-Alkali Plants - Air Streams | |
| Method 101A - Determination of Particulate and Gaseous Mercury Emissions from Stationary Sources | |
| Method 102 - Determination of Particulate and Gaseous Mercury Emissions from Chlor-Alkali Plants - Hydrogen Streams | |
| Method 103 - Beryllium Screening Method | |
| Method 104 - Determination of Beryllium Emissions from Stationary Sources | |
| Method 105 - Determination of Mercury in Wastewater Treatment Plant Sewage Sludge | |
| Method 106 - Determination of Vinyl Chloride from Stationary Sources | |
| Method 107 - Determination of Vinyl Chloride Content of Process Stream Samples | |
| Method 107A - Determination of Vinyl Chloride Content of Solvents, Resin-Solvent Solution, Polyvinyl Chloride Resin, Resin Slurry, Wet Resin, and Latex Samples | |
| Method 108 - Determination of Particulate and Gaseous Arsenic Emissions | |
| Method 108A - Determination of Arsenic Content in Ore Samples from Nonferrous Smelters | |
| Method 108B - Determination of Arsenic Content in Ore Samples from Nonferrous Smelters | |
| Method 108C - Determination of Arsenic Content in Ore Samples from Nonferrous Smelters | |
| Method 200 - Determination of Total Particulate, Free Chlorine, and Total Chlorides from Secondary Aluminum Smelters and Other Stationary Sources | |
| Method 201 - Determination of PM10 Emissions (Exhaust Gas Recycle Procedure) | |
| Method 201A - Determination of PM10 Emissions (Constant Sampling Rate Procedure) | |
| Method 202 - Determination of Condensible Particulate Emissions from Stationary Sources | |
| Method 204 - Criteria for and Verification of a Permanent or Temporary Total Enclosure | |
| Method 204A - Volatile Organic Compounds Content in Liquid Input Stream | |
| Method 204B - Volatile Organic Compounds Emissions in Capture Stream | |
| Method 204C - Volatile Organic Compounds Emissions in Captured Stream (Dilution Technique) | |
| Method 204D - Volatile Organic Compounds Emissions in Fugitive Stream from Temporary Total Enclosure | |
| Method 204E - Volatile Organic Compounds Emissions in Fugitive Stream from Building Enclosure | |
| Method 204F - Volatile Organic Compounds Content in Liquid Input Stream (Distillation Approach) | |
| Method 300 - Determination of Surface Coating Transfer Efficiency | |
| Method 301 - Field Validation of Pollutant Measurement Methods from Various Waste Media | |
| Method 304A - Determination of Biodegradation Rates of Organic Compounds (Vent Option) | |
| Method 304B - Determination of Rates of Organic Compounds (Scrubber Option) | |
| Method 305 - Measurement of Emission Potential of Individual Volatile Organic Compounds in Waste | |
| Method 306 - Determination of Chromium Emissions from Decorative and Hard Chromium Electroplating and Anodizing Operations | |
| Method 306A - Determination of Chromium Emissions from Decorative and Hard Chromium Electroplating and Anodizing Operations | |
| Method 306B - Surface Tension Measurement and Recordkeeping for Chromium Plating Tanks Used at Electroplating and Anodizing Facilities | |
| Method 307 - Determination of Emissions from Halogenated Solvent Vapor Cleaning Machines using a Liquid Level Procedure | |
| Method 308 - Procedure for Determination of Methanol Emissions from Stationary Sources | |
| Method 310A - Determination of Residual Hexane through Gas Chromatography | |
| Method 310B - Determination of Residual Solvent through Gas Chromatography | |
| Method 310C - Determination of Residual N-Hexane in EPDM Rubber through Gas Chromatography | |
| Method 311 - Analysis of Hazardous Air Pollutant Compounds in Paints and Coatings by Direct Injection into a Gas Chromatograph | |
| Method 312A - Determination of Styrene in Latex Styrene-Butadiene Rubber through Gas Chromatography | |
| Method 312B - Determination of Residual Styrene in Styrene-Butadiene (SBR) Rubber Latex by Capillary Gas Chromatography | |
| Method 312C - Determination of Residual Styrene in SBR Latex Produced by Emulsion Polymerization | |
| Method 313A - Determination of Residual Hydrocarbons in Rubber Crumb | |
| Method 313B - The Determination of Residual Hydrocarbon in Solution Polymers by Capillary Gas Chromatography | |
| Method 316 - Sampling and Analysis for Formaldehyde Emissions from Stationary Sources in the Mineral Wool and Wool Fiberglass Industries | |
| Appendix A - Part II - Field Data Sheets | |
| Appendix B - Continuous Emission Monitor Performance Specifications | |
| PS 1 - Specifications and Test Procedures for Opacity Continuous Emission Monitoring Systems in Stationary Sources | |
| PS 2 - Specifications and Test Procedures for SO2 and NOx Continuous Emission Monitoring Systems in Stationary Sources | |
| PS 3 - Specifications and Test Procedures for O2 and CO2 Continuous Emission Monitoring Systems in Stationary Sources | |
| PS 4 - Specifications and Test Procedures for Carbon Monoxide Continuous Emission Monitoring Systems in Stationary Sources | |
| PS 4A - Specifications and Test Procedures for Carbon Monoxide Continuous Emission Monitoring Systems in Stationary Sources | |
| PS 5 - Specifications and Test Procedures for TRS Continuous Emission Monitoring Systems in Stationary Sources | |
| PS 7 - Specifications and Test Procedures for Hydrogen Sulfide Continuous Emission Monitoring Systems in Stationary Sources | |
| PS 12A - Specifications and Test Procedures for Total Vapor Phase Mercury Continuous Emission Monitoring Systems in Stationary Sources | |
| Appendix C - Quality Assurance Procedures for Gas Chromatography: | |
| Procedure 1 - Determination of Adequate Chromatographic Peak Resolution | |
| Procedure 2 - Procedure for Field Auditing GC Analysis | |
| Appendix D - Determination of Emission Rate Change | |
| Appendix E - Performance Specifications for Flow Monitors | |
| Performance Specifications and Specification Test Procedures for Monitoring Systems for Effluent Stream Gas Volumetric Flow Rate | |
| Appendix F - Quality Assurance Procedures | |
| Procedure 1 - Quality Assurance Requirements for Gas Continuous Emission Monitoring Systems Used for Compliance Determination | |
| Appendix G | |
| Protocols for Determining VOC Capture Efficiency | |
| Appendix H | |
| Calculation of VOC Emissions from Open Molding Fiber-Reinforced Plastics Manufacturing | |
| [Note: Unified Emission Factors (UEF) for Open Molding of Composites is given as a separate pdf.] | |
| Appendix I | |
| Performance Test Calculations and Reporting | |
| PART V : Bibliography | |
| **Proposed changes to the Test Manual |
|
| Table of Contents | |
| Section 2.124 - Multipollutant Control for Electric Utility Steam Generating Units | |
| Method 16C - Determination of Total Reduced Sulfur Emissions from Stationary Sources (Instrumental Analyzer Procedure | |
| Method 201A - Determination of Determination of PM10 and PM2.5 Emissions from Stationary Sources (Constant Sampling Rate Procedure) | |
| Method 202 - Dry Impinger Method for Determining Condensable Particulate Emissions from Stationary Sources | |
| Appendix B PS 6 - Specifications and Test Procedures for Continuous Emission Rate Monitoring Systems in Stationary Sources | |
| Appendix B PS 11 - Specifications and Test Procedures for Particulate Matter Continuous Emission Monitoring Systems at Stationary Sources | |
| Appendix B PS 12A - Specifications and Test Procedures for Total Vapor Phase Mercury Continuous Emission Monitoring Systems in Stationary Sources | |
| Appendix F Procedure 2 - Quality Assurance Requirements for Particulate Matter Continuous Emission Monitoring Systems at Stationary Sources | |
Proposed changes to the Test Manual may be found at
the end of this document